反應(ying)釜(fu)清洗(xi)(xi)要(yao)求：1、將反應(ying)溶(rong)劑(ji)從排氣(qi)閥(fa)充(chong)(chong)入(ru)釜(fu)內(nei)(nei)(nei)，清洗(xi)(xi)掉大部份殘留物后，注(zhu)入(ru)水半釜(fu)進(jin)行攪拌10分鐘，此時(shi)(shi)方(fang)可(ke)打開(kai)釜(fu)蓋(gai)，對(dui)釜(fu)內(nei)(nei)(nei)壁進(jin)行清洗(xi)(xi)。2、清洗(xi)(xi)時(shi)(shi)，必須清洗(xi)(xi)釜(fu)蓋(gai)、取樣(yang)閥(fa)，同時(shi)(shi)在釜(fu)內(nei)(nei)(nei)有(you)水的(de)情況下，稍充(chong)(chong)一下氮氣(qi)。3、暫時(shi)(shi)不用的(de)反應(ying)釜(fu)，將反應(ying)釜(fu)內(nei)(nei)(nei)加入(ru)70%體積干凈(jing)的(de)無(wu)水乙醇浸泡，可(ke)以(yi)不擰緊螺絲。高(gao)壓釜(fu)清洗(xi)(xi)完后，方(fang)可(ke)方(fang)便(bian)下次使用。3. 隔套上部裝有(you)測速(su)(su)線(xian)圈(quan)，連(lian)成一體的(de)攪拌器(qi)(qi)與內(nei)(nei)(nei)磁環旋(xuan)轉時(shi)(shi)，測速(su)(su)線(xian)圈(quan)便(bian)產生感應(ying)電動勢(shi)，該電勢(shi)與攪拌轉速(su)(su)相(xiang)應(ying)，該電勢(shi)傳遞(di)到轉速(su)(su)表(biao)上，便(bian)可(ke)顯示出攪拌轉速(su)(su)。4. 軸(zhou)承采用不銹鋼軸(zhou)承或高(gao)強電化(hua)石墨，耐摩損，且維修周期長。1. 反應(ying)釜(fu)主密封(feng)口(kou)采用A型的(de)雙線(xian)密封(feng)，其余密封(feng)點均采用圓弧面(mian)與平面(mian)、圓弧面(mian)與圓弧面(mian)的(de)線(xian)接觸(chu)的(de)密封(feng)形式，依靠接觸(chu)面(mian)的(de)高(gao)精度(du)和光潔度(du)，達到良好的(de)密封(feng)效果。2. 釜(fu)蓋(gai)上裝有(you)壓力表(biao)，膜安全裝置(zhi)，汽液相(xiang)閥(fa)，溫度(du)傳感器(qi)(qi)等，便(bian)于隨(sui)時(shi)(shi)了(le)解釜(fu)內(nei)(nei)(nei)的(de)反應(ying)情況，調節(jie)釜(fu)內(nei)(nei)(nei)的(de)介質比例，并確保安全運行。

智能高(gao)壓(ya)(ya)(ya)(ya)反(fan)(fan)應(ying)釜(fu)(fu)：磁力(li)(li)傳動(dong)裝置是高(gao)壓(ya)(ya)(ya)(ya)反(fan)(fan)應(ying)器(qi)實(shi)(shi)現物(wu)料混(hun)合的(de)技(ji)術，是設(she)計壓(ya)(ya)(ya)(ya)力(li)(li)超過50bar的(de)必(bi)須(xu)部(bu)件(jian)。公開后(hou)成(cheng)為(wei)(wei)壓(ya)(ya)(ya)(ya)混(hun)合設(she)備(bei)的(de)行(xing)業標準(zhun)。使用實(shi)(shi)驗(yan)室高(gao)壓(ya)(ya)(ya)(ya)反(fan)(fan)應(ying)釜(fu)(fu)有(you)哪些注(zhu)意事(shi)項(xiang):水壓(ya)(ya)(ya)(ya)試(shi)(shi)驗(yan)后(hou)，再可進(jin)密試(shi)(shi)驗(yan)。1．氣(qi)密試(shi)(shi)驗(yan)壓(ya)(ya)(ya)(ya)力(li)(li)為(wei)(wei)我作壓(ya)(ya)(ya)(ya)力(li)(li)。2．氣(qi)密試(shi)(shi)驗(yan)的(de)介(jie)質為(wei)(wei)氮氣(qi)或者其它惰性氣(qi)體。3．氣(qi)密試(shi)(shi)驗(yan)時(shi)(shi)，升壓(ya)(ya)(ya)(ya)必(bi)須(xu)分次進(jin)行(xing)。達(da)到壓(ya)(ya)(ya)(ya)力(li)(li)后(hou)，保(bao)壓(ya)(ya)(ya)(ya)一定時(shi)(shi)間，用肥皂(zao)水檢(jian)查(cha)有(you)無泄漏，合格后(hou)緩(huan)(huan)緩(huan)(huan)泄壓(ya)(ya)(ya)(ya)。 使用實(shi)(shi)驗(yan)室高(gao)壓(ya)(ya)(ya)(ya)反(fan)(fan)應(ying)釜(fu)(fu)有(you)哪些注(zhu)意事(shi)項(xiang); 1.安(an)裝前(qian)，首先(xian)檢(jian)查(cha)各聯(lian)接件(jian)、緊固件(jian)及傳動(dong)部(bu)位是否牢固可靠。 2.安(an)裝時(shi)(shi)，要底(di)座與地水平(ping)垂(chui)直，工業高(gao)壓(ya)(ya)(ya)(ya)反(fan)(fan)應(ying)釜(fu)(fu)，不垂(chui)直度(du)不得大于設(she)備(bei)總高(gao)度(du)的(de)1/1000。3.壓(ya)(ya)(ya)(ya)力(li)(li)表、安(an)全閥、法(fa)蘭等(deng)配(pei)件(jian)必(bi)須(xu)按反(fan)(fan)應(ying)釜(fu)(fu)工作壓(ya)(ya)(ya)(ya)力(li)(li)要求配(pei)備(bei)。4.設(she)備(bei)安(an)放應(ying)遠離強磁場、電爐等(deng)較大的(de)用電設(she)備(bei)。 5.檢(jian)查(cha)線路有(you)沒有(you)接地短(duan)路等(deng)現象。6. 工作時(shi)(shi)禁止運(yun)輸，停止工作后(hou)運(yun)輸中不允許把反(fan)(fan)應(ying)器(qi)放倒(dao)或側臥運(yun)輸。

使(shi)(shi)(shi)用(yong)(yong)(yong)(yong)(yong)實驗(yan)(yan)室高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜有(you)哪些注(zhu)意事項:水(shui)壓(ya)(ya)(ya)(ya)(ya)試(shi)驗(yan)(yan) 1．安(an)裝(zhuang)完畢后(hou)進行(xing)水(shui)壓(ya)(ya)(ya)(ya)(ya)試(shi)驗(yan)(yan)，水(shui)壓(ya)(ya)(ya)(ya)(ya)試(shi)驗(yan)(yan)按1.05倍(bei)工作壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)試(shi)驗(yan)(yan)。 2．要求裝(zhuang)配(pei)量(liang)(liang)程為工作壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)的(de)(de)(de)(de)1.25倍(bei)的(de)(de)(de)(de)合(he)格壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)表 3．用(yong)(yong)(yong)(yong)(yong)清(qing)潔(jie)水(shui)作介質(zhi)，確認(ren)氯離子含量(liang)(liang)不超過(guo)25毫克/升(sheng)，大型高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜，水(shui)溫(wen)(wen)(wen)≥5°C。4．充介質(zhi)時，容(rong)器(qi)(qi)(qi)頂部(bu)設排氣口(kou)，必須把容(rong)器(qi)(qi)(qi)內(nei)部(bu)的(de)(de)(de)(de)氣體(ti)排放(fang)干凈。5．試(shi)壓(ya)(ya)(ya)(ya)(ya)時，壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)應(ying)(ying)(ying)(ying)緩(huan)慢上(shang)(shang)升(sheng)，注(zhu)意觀察壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)指示是否變化，湖北高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜，容(rong)器(qi)(qi)(qi)有(you)無變形，傾聽有(you)無異常聲響，實驗(yan)(yan)室高(gao)(gao)溫(wen)(wen)(wen)高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜，達到(dao)試(shi)驗(yan)(yan)壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)保(bao)壓(ya)(ya)(ya)(ya)(ya)30分鐘(zhong)。無泄(xie)漏后(hou)，將壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)緩(huan)緩(huan)降到(dao)試(shi)驗(yan)(yan)壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)的(de)(de)(de)(de)80%；保(bao)壓(ya)(ya)(ya)(ya)(ya)一定(ding)時間(jian)，對所有(you)的(de)(de)(de)(de)接(jie)頭和(he)連接(jie)部(bu)位(wei)進行(xing)檢查。合(he)格后(hou)緩(huan)緩(huan)缷壓(ya)(ya)(ya)(ya)(ya)，放(fang)盡介質(zhi)，用(yong)(yong)(yong)(yong)(yong)壓(ya)(ya)(ya)(ya)(ya)縮(suo)空氣將容(rong)器(qi)(qi)(qi)內(nei)外吹干凈。注(zhu)意事項：高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜要在的(de)(de)(de)(de)地(di)點使(shi)(shi)(shi)用(yong)(yong)(yong)(yong)(yong)，并按照使(shi)(shi)(shi)用(yong)(yong)(yong)(yong)(yong)說明(ming)(ming)進行(xing)操(cao)(cao)作。查明(ming)(ming)刻于(yu)主體(ti)容(rong)器(qi)(qi)(qi)上(shang)(shang)的(de)(de)(de)(de)試(shi)驗(yan)(yan)壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)、使(shi)(shi)(shi)用(yong)(yong)(yong)(yong)(yong)壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)及(ji)使(shi)(shi)(shi)用(yong)(yong)(yong)(yong)(yong)溫(wen)(wen)(wen)度等(deng)條(tiao)件(jian)，要在其容(rong)許的(de)(de)(de)(de)條(tiao)件(jian)范圍內(nei)進行(xing)使(shi)(shi)(shi)用(yong)(yong)(yong)(yong)(yong)。高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜的(de)(de)(de)(de)操(cao)(cao)作及(ji)注(zhu)意事項：4、氧氣壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)計應(ying)(ying)(ying)(ying)避免(mian)與其他氣體(ti)壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)計混合(he)。5、安(an)全閥和(he)其他安(an)全裝(zhuang)置應(ying)(ying)(ying)(ying)定(ding)期(qi)檢查符(fu)合(he)要求的(de)(de)(de)(de)設備。6、操(cao)(cao)作時必須注(zhu)意溫(wen)(wen)(wen)度計應(ying)(ying)(ying)(ying)準確插入反(fan)應(ying)(ying)(ying)(ying)溶(rong)液。7、保(bao)持高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜內(nei)部(bu)和(he)墊片清(qing)潔(jie)。8、蓋(gai)上(shang)(shang)盤(pan)式(shi)法蘭蓋(gai)時，位(wei)于(yu)對角(jiao)線上(shang)(shang)的(de)(de)(de)(de)螺栓應(ying)(ying)(ying)(ying)依次擰緊(jin)。9、測量(liang)(liang)儀器(qi)(qi)(qi)時，大多數情(qing)況下玻(bo)璃(li)表面前后(hou)兩側。所以操(cao)(cao)作時不要站在這些危(wei)險的(de)(de)(de)(de)地(di)方。當(dang)預計有(you)危(wei)險時，卸下玻(bo)璃(li)，換上(shang)(shang)新的(de)(de)(de)(de)。