注(zhu)(zhu)意(yi)事項：壓(ya)(ya)(ya)(ya)(ya)力(li)(li)計(ji)(ji)(ji)所(suo)使(shi)(shi)(shi)用(yong)(yong)(yong)的壓(ya)(ya)(ya)(ya)(ya)力(li)(li)，好(hao)在其標明壓(ya)(ya)(ya)(ya)(ya)力(li)(li)的1/2以(yi)(yi)(yi)內(nei)使(shi)(shi)(shi)用(yong)(yong)(yong)。并經(jing)常把壓(ya)(ya)(ya)(ya)(ya)力(li)(li)計(ji)(ji)(ji)與(yu)標準壓(ya)(ya)(ya)(ya)(ya)力(li)(li)計(ji)(ji)(ji)進行(xing)比較，加以(yi)(yi)(yi)校(xiao)正。氧氣(qi)用(yong)(yong)(yong)的壓(ya)(ya)(ya)(ya)(ya)力(li)(li)計(ji)(ji)(ji)，要(yao)(yao)(yao)避免與(yu)其它氣(qi)體用(yong)(yong)(yong)的壓(ya)(ya)(ya)(ya)(ya)力(li)(li)計(ji)(ji)(ji)混用(yong)(yong)(yong)。安(an)全(quan)閥及其它的安(an)全(quan)裝置，要(yao)(yao)(yao)使(shi)(shi)(shi)用(yong)(yong)(yong)經(jing)過定(ding)期檢查符合規(gui)定(ding)要(yao)(yao)(yao)求(qiu)的器械。操作(zuo)時(shi)(shi)必須注(zhu)(zhu)意(yi)，溫度計(ji)(ji)(ji)要(yao)(yao)(yao)準確的插到(dao)反(fan)(fan)(fan)應(ying)(ying)溶液中。高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)發應(ying)(ying)釜(fu)適用(yong)(yong)(yong)范(fan)圍，高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)釜(fu)即(ji)高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)(fan)(fan)應(ying)(ying)釜(fu)，適用(yong)(yong)(yong)于大專院校(xiao)實(shi)(shi)驗(yan)、石(shi)油化工(gong)、染料礦冶(ye)、納米材料、聚合物(wu)(wu)反(fan)(fan)(fan)應(ying)(ying)、水熱合成(cheng)、氫化反(fan)(fan)(fan)應(ying)(ying)、科技(ji)、食品(pin)、卷煙業、陶瓷業、高(gao)(gao)(gao)分(fen)子業、精細化工(gong)、微生(sheng)物(wu)(wu)工(gong)程(cheng)、高(gao)(gao)(gao)新科技(ji)產品(pin)等領域使(shi)(shi)(shi)用(yong)(yong)(yong)實(shi)(shi)驗(yan)室高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)(fan)(fan)應(ying)(ying)釜(fu)有哪(na)些注(zhu)(zhu)意(yi)事項：前用(yong)(yong)(yong)軟布擦干凈，不(bu)能有雜質影響密封(feng)，操作(zuo)時(shi)(shi)要(yao)(yao)(yao)注(zhu)(zhu)意(yi)保(bao)護上緊主(zhu)螺栓時(shi)(shi)不(bu)可用(yong)(yong)(yong)力(li)(li)過猛，不(bu)得超過擰(ning)緊力(li)(li)矩(ju)范(fan)圍80~120N.M；且應(ying)(ying)按(an)對角分(fen)布原則，均(jun)勻對稱(cheng)地上緊螺栓，分(fen)2~3次擰(ning)緊，以(yi)(yi)(yi)防(fang)止擠壞(huai)密封(feng)面(mian)。組裝時(shi)(shi)，要(yao)(yao)(yao)輕(qing)拿輕(qing)放，防(fang)止密封(feng)面(mian)相互撞(zhuang)擊，不(bu)允許硬物(wu)(wu)碰撞(zhuang)密封(feng)部分(fen)，以(yi)(yi)(yi)免損壞(huai)密封(feng)面(mian)而導致(zhi)泄漏(lou)。若使(shi)(shi)(shi)用(yong)(yong)(yong)合理，高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)(fan)(fan)應(ying)(ying)釜(fu)，可使(shi)(shi)(shi)用(yong)(yong)(yong)千(qian)次以(yi)(yi)(yi)上。密封(feng)面(mian)損傷后(hou)，要(yao)(yao)(yao)重新整修拋光后(hou)，方可恢復密封(feng)性能。上述(shu)工(gong)作(zuo)完成(cheng)后(hou)，實(shi)(shi)驗(yan)室高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)(fan)(fan)應(ying)(ying)釜(fu)多少錢，按(an)設計(ji)(ji)(ji)壓(ya)(ya)(ya)(ya)(ya)力(li)(li)進行(xing)水壓(ya)(ya)(ya)(ya)(ya)試(shi)驗(yan)與(yu)氣(qi)密性試(shi)驗(yan)，介質為去離(li)子水、氮(dan)氣(qi)或者其它惰(duo)性氣(qi)體，嚴禁(jin)使(shi)(shi)(shi)用(yong)(yong)(yong)氣(qi)體，小型高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)(fan)(fan)應(ying)(ying)釜(fu)，升壓(ya)(ya)(ya)(ya)(ya)必須分(fen)次進行(xing)，保(bao)壓(ya)(ya)(ya)(ya)(ya)15~30分(fen)鐘，不(bu)得有泄漏(lou)，發現漏(lou)氣(qi)應(ying)(ying)后(hou)修復再(zai)試(shi)驗(yan)。

使用(yong)實(shi)驗室高(gao)壓反(fan)(fan)應(ying)(ying)(ying)釜(fu)有(you)哪些注意事項:序號(hao) 故障現象(xiang) 可能原因 排除(chu)方(fang)法 1 打開(kai)(kai)上(shang)(shang)電(dian)(dian)源(yuan)(yuan)開(kai)(kai)關(guan)(guan)但控制面板(ban)(ban)不亮 1.總電(dian)(dian)源(yuan)(yuan)保(bao)險(xian)(xian)絲損(sun)壞(huai)(huai)。2.電(dian)(dian)源(yuan)(yuan)開(kai)(kai)關(guan)(guan)內部(bu)接(jie)觸(chu)不良(liang)。3.接(jie)電(dian)(dian)電(dian)(dian)源(yuan)(yuan)有(you)誤。 1. 更(geng)(geng)(geng)換(huan)(huan)保(bao)險(xian)(xian)絲。2. 更(geng)(geng)(geng)換(huan)(huan)開(kai)(kai)關(guan)(guan)。3. 用(yong)表測(ce)量所(suo)使用(yong)的(de)電(dian)(dian)源(yuan)(yuan)電(dian)(dian)壓并作更(geng)(geng)(geng)正。 2 液晶屏(ping)上(shang)(shang)排顯示(shi)“----”， 1. 溫(wen)度(du)傳(chuan)感(gan)(gan)器(qi)(qi)插(cha)頭(tou)沒插(cha)，2. 溫(wen)度(du)傳(chuan)感(gan)(gan)器(qi)(qi)連(lian)接(jie)線(xian)損(sun)壞(huai)(huai)。3. 主板(ban)(ban)失靈(ling)。 1. 插(cha)上(shang)(shang)溫(wen)度(du)傳(chuan)感(gan)(gan)器(qi)(qi)插(cha)頭(tou)。2. 更(geng)(geng)(geng)換(huan)(huan)溫(wen)度(du)傳(chuan)感(gan)(gan)器(qi)(qi)連(lian)接(jie)線(xian)。3. 更(geng)(geng)(geng)換(huan)(huan)主板(ban)(ban)。 3 液晶屏(ping)下排顯示(shi)“E-1”且馬達不工作 1. 介質(zhi)很粘稠(chou)至攪拌受阻2. 軟軸(zhou)受阻 1. 檢查介質(zhi)是否很粘稠(chou)；2. 重新拆裝(zhuang)(zhuang)(zhuang)軟軸(zhou)。 4 打開(kai)(kai)開(kai)(kai)關(guan)(guan)即(ji)燒(shao)保(bao)險(xian)(xian)絲或更(geng)(geng)(geng)換(huan)(huan)保(bao)險(xian)(xian)絲后馬上(shang)(shang)燒(shao)斷。 1. 加(jia)熱器(qi)(qi)燒(shao)壞(huai)(huai)短(duan)路。2. 主板(ban)(ban)燒(shao)壞(huai)(huai) 1. 更(geng)(geng)(geng)換(huan)(huan)加(jia)熱器(qi)(qi)。2. 更(geng)(geng)(geng)換(huan)(huan)主板(ban)(ban)。 5 溫(wen)度(du)、攪拌速度(du)無(wu)法控制。 1. 主板(ban)(ban)燒(shao)壞(huai)(huai)。 1.更(geng)(geng)(geng)換(huan)(huan)主板(ban)(ban)。高(gao)壓反(fan)(fan)應(ying)(ying)(ying)釜(fu)的(de)自(zi)潤滑軸(zhou)套耐高(gao)溫(wen)高(gao)壓、耐腐蝕耐磨擦、避免了(le)(le)二(er)次污染從(cong)而保(bao)證了(le)(le)物料純度(du)，適合氣體(ti)(ti) / 液體(ti)(ti) / 固體(ti)(ti)混合、懸浮、對流、較大粘度(du)物料、高(gao)轉速攪拌反(fan)(fan)應(ying)(ying)(ying)。高(gao)壓釜(fu)所(suo)有(you)密(mi)(mi)(mi)封(feng)(feng)部(bu)位采用(yong)線(xian)密(mi)(mi)(mi)封(feng)(feng)因而整體(ti)(ti)設備不存在泄漏問題，有(you)上(shang)(shang)下兩種(zhong)進排料方(fang)式(shi)，縮(suo)短(duan)了(le)(le)攪拌時間、強化了(le)(le)反(fan)(fan)應(ying)(ying)(ying)過程，是開(kai)(kai)發試驗產(chan)品(pin)的(de)裝(zhuang)(zhuang)(zhuang)置。注意事項：高(gao)壓釜(fu)屬于精密(mi)(mi)(mi)設備，通過密(mi)(mi)(mi)封(feng)(feng)環采用(yong)錐(zhui)面相(xiang)接(jie)觸(chu)密(mi)(mi)(mi)封(feng)(feng)形式(shi)，借(jie)擰(ning)緊主螺(luo)栓(shuan)使他們相(xiang)互壓緊而達到密(mi)(mi)(mi)封(feng)(feng)的(de)目的(de)。必須對密(mi)(mi)(mi)封(feng)(feng)錐(zhui)面特別加(jia)以(yi)愛護，避免各種(zhong)碰撞而導致(zhi)其損(sun)壞(huai)(huai)。在裝(zhuang)(zhuang)(zhuang)蓋(gai)時，先放置好反(fan)(fan)應(ying)(ying)(ying)釜(fu)釜(fu)體(ti)(ti)，然后將(jiang)釜(fu)蓋(gai)按(an)(an)固定(ding)位置，小心地(di)裝(zhuang)(zhuang)(zhuang)在釜(fu)體(ti)(ti)上(shang)(shang)，在擰(ning)緊主螺(luo)栓(shuan)時，必須按(an)(an)對角，對稱地(di)分多(duo)次逐步擰(ning)緊，用(yong)力要(yao)均勻，不允許(xu)釜(fu)蓋(gai)向一邊傾斜，以(yi)達到良(liang)好的(de)密(mi)(mi)(mi)封(feng)(feng)效果，不可超(chao)過規定(ding)之(zhi)擰(ning)緊力矩，以(yi)防密(mi)(mi)(mi)封(feng)(feng)面被擠壞(huai)(huai)或加(jia)速磨損(sun)。

高(gao)壓(ya)反(fan)(fan)應(ying)釜(fu)(磁力(li)高(gao)壓(ya)反(fan)(fan)應(ying)釜(fu))是(shi)磁力(li)傳動裝置應(ying)用于反(fan)(fan)應(ying)設備的(de)(de)典型(xing)創(chuang)新，高(gao)壓(ya)實驗(yan)反(fan)(fan)應(ying)釜(fu)，它(ta)(ta)從(cong)根本上解決(jue)了以(yi)前(qian)填料密(mi)(mi)封(feng)、機(ji)(ji)械密(mi)(mi)封(feng)無(wu)(wu)法克服(fu)的(de)(de)軸(zhou)封(feng)泄(xie)(xie)漏問題，在(zai)化工業方面的(de)(de)使用非(fei)常(chang)常(chang)見，我(wo)們在(zai)使用的(de)(de)時候也需要小心高(gao)壓(ya)反(fan)(fan)應(ying)釜(fu)（磁力(li)高(gao)壓(ya)反(fan)(fan)應(ying)釜(fu)）是(shi)磁力(li)傳動裝置應(ying)用于反(fan)(fan)應(ying)設備的(de)(de)典型(xing)創(chuang)新，它(ta)(ta)從(cong)根本上解決(jue)了以(yi)前(qian)填料密(mi)(mi)封(feng)、機(ji)(ji)械密(mi)(mi)封(feng)無(wu)(wu)法克服(fu)的(de)(de)軸(zhou)封(feng)泄(xie)(xie)漏問題，無(wu)(wu)任何泄(xie)(xie)漏和污染，是(shi)國(guo)內進(jin)行高(gao)溫(wen)、高(gao)壓(ya)下(xia)的(de)(de)化學反(fan)(fan)應(ying)為理想的(de)(de)裝置，特(te)別是(shi)進(jin)行、、有毒(du)介質的(de)(de)化學反(fan)(fan)應(ying)，更(geng)加顯示(shi)出它(ta)(ta)的(de)(de)性。使用實驗(yan)室高(gao)壓(ya)反(fan)(fan)應(ying)釜(fu)有哪些注意事項(xiang):水(shui)壓(ya)試(shi)驗(yan)后，再可進(jin)密(mi)(mi)試(shi)驗(yan)。1．氣密(mi)(mi)試(shi)驗(yan)壓(ya)力(li)為我(wo)作壓(ya)力(li)。2．氣密(mi)(mi)試(shi)驗(yan)的(de)(de)介質為氮(dan)氣或者(zhe)其它(ta)(ta)惰(duo)性氣體。3．氣密(mi)(mi)試(shi)驗(yan)時，升壓(ya)必須分(fen)次進(jin)行。達到壓(ya)力(li)后，保壓(ya)一定(ding)時間，用肥皂水(shui)檢(jian)查有無(wu)(wu)泄(xie)(xie)漏，合(he)格后緩(huan)緩(huan)泄(xie)(xie)壓(ya)。