反應釜清洗要求：1、將反應溶劑從排氣閥充入釜內，清洗掉大部份殘留物后，注入水半釜進行攪拌10分鐘，此時方可打開釜蓋，吉林高壓反應釜，對釜內壁進行清洗。2、清洗時，必須清洗釜蓋、取樣閥，同時在釜內有水的情況下，稍充一下氮氣。3、暫時不用的反應釜，將反應釜內加入70%體積干凈的無水乙醇浸泡，可以不擰緊螺絲。高壓釜清洗完后，方可方便下次使用。高壓反應釜的壓力范圍是多大：如果反應釜符合壓力容器的規定即為壓力容器，按壓力等級分為壓力容器可分為內壓容器與外壓容器。內壓容器又可按設計壓力(p)大小分為四個壓力等級1.低壓(代號L)容器0.1MPa≤p

高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)反(fan)(fan)(fan)(fan)應(ying)(ying)(ying)釜(磁力(li)高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)反(fan)(fan)(fan)(fan)應(ying)(ying)(ying)釜)是(shi)磁力(li)傳動裝置(zhi)應(ying)(ying)(ying)用于(yu)反(fan)(fan)(fan)(fan)應(ying)(ying)(ying)設備的(de)典型(xing)創(chuang)新，它(ta)(ta)從(cong)根(gen)本上(shang)(shang)解決(jue)了以(yi)前(qian)填(tian)料密(mi)(mi)(mi)(mi)封(feng)、機(ji)械(xie)(xie)密(mi)(mi)(mi)(mi)封(feng)無法克服(fu)的(de)軸封(feng)泄(xie)(xie)漏問題(ti)(ti)，在化(hua)工業(ye)方面的(de)使用非常常見(jian)，我(wo)們在使用的(de)時候也需要小(xiao)心高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)反(fan)(fan)(fan)(fan)應(ying)(ying)(ying)釜（磁力(li)高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)反(fan)(fan)(fan)(fan)應(ying)(ying)(ying)釜）是(shi)磁力(li)傳動裝置(zhi)應(ying)(ying)(ying)用于(yu)反(fan)(fan)(fan)(fan)應(ying)(ying)(ying)設備的(de)典型(xing)創(chuang)新，它(ta)(ta)從(cong)根(gen)本上(shang)(shang)解決(jue)了以(yi)前(qian)填(tian)料密(mi)(mi)(mi)(mi)封(feng)、機(ji)械(xie)(xie)密(mi)(mi)(mi)(mi)封(feng)無法克服(fu)的(de)軸封(feng)泄(xie)(xie)漏問題(ti)(ti)，無任何泄(xie)(xie)漏和污染(ran)，是(shi)國內進行(xing)高(gao)(gao)(gao)溫、高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)下的(de)化(hua)學(xue)反(fan)(fan)(fan)(fan)應(ying)(ying)(ying)為(wei)理想(xiang)的(de)裝置(zhi)，特別是(shi)進行(xing)、、有(you)(you)毒介質的(de)化(hua)學(xue)反(fan)(fan)(fan)(fan)應(ying)(ying)(ying)，更加顯示出它(ta)(ta)的(de)性(xing)。使用實驗(yan)(yan)(yan)室高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)反(fan)(fan)(fan)(fan)應(ying)(ying)(ying)釜有(you)(you)哪些注意事項:水壓(ya)(ya)(ya)(ya)試(shi)驗(yan)(yan)(yan)后，再可進密(mi)(mi)(mi)(mi)試(shi)驗(yan)(yan)(yan)。1．氣(qi)密(mi)(mi)(mi)(mi)試(shi)驗(yan)(yan)(yan)壓(ya)(ya)(ya)(ya)力(li)為(wei)我(wo)作(zuo)壓(ya)(ya)(ya)(ya)力(li)。2．氣(qi)密(mi)(mi)(mi)(mi)試(shi)驗(yan)(yan)(yan)的(de)介質為(wei)氮氣(qi)或(huo)者(zhe)其它(ta)(ta)惰性(xing)氣(qi)體。3．氣(qi)密(mi)(mi)(mi)(mi)試(shi)驗(yan)(yan)(yan)時，升壓(ya)(ya)(ya)(ya)必須分次進行(xing)。達到壓(ya)(ya)(ya)(ya)力(li)后，保壓(ya)(ya)(ya)(ya)一定時間(jian)，用肥(fei)皂水檢(jian)查有(you)(you)無泄(xie)(xie)漏，合格后緩(huan)緩(huan)泄(xie)(xie)壓(ya)(ya)(ya)(ya)。

注(zhu)意(yi)事(shi)(shi)項：高壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)釜(fu)(fu)屬于(yu)精密(mi)(mi)設備，通過(guo)密(mi)(mi)封(feng)環采用(yong)(yong)(yong)錐面(mian)相接觸密(mi)(mi)封(feng)形式，借擰(ning)(ning)緊(jin)(jin)主螺栓(shuan)使(shi)(shi)(shi)他們相互壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)緊(jin)(jin)而達到密(mi)(mi)封(feng)的(de)(de)(de)目的(de)(de)(de)。必(bi)須對密(mi)(mi)封(feng)錐面(mian)特(te)別加(jia)以(yi)愛護，避(bi)免(mian)各種碰撞(zhuang)而導致其(qi)損(sun)壞。在裝蓋時(shi)，先放置(zhi)(zhi)好(hao)反(fan)(fan)應(ying)(ying)(ying)釜(fu)(fu)釜(fu)(fu)體，然(ran)后將(jiang)釜(fu)(fu)蓋按(an)固(gu)定(ding)(ding)位置(zhi)(zhi)，小(xiao)(xiao)心地(di)(di)裝在釜(fu)(fu)體上，在擰(ning)(ning)緊(jin)(jin)主螺栓(shuan)時(shi)，必(bi)須按(an)對角，對稱地(di)(di)分多次(ci)逐(zhu)步擰(ning)(ning)緊(jin)(jin)，小(xiao)(xiao)型(xing)高壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)反(fan)(fan)應(ying)(ying)(ying)釜(fu)(fu)，用(yong)(yong)(yong)力(li)(li)(li)要(yao)(yao)均勻(yun)，不(bu)允許釜(fu)(fu)蓋向(xiang)一邊傾斜(xie)，以(yi)達到良(liang)好(hao)的(de)(de)(de)密(mi)(mi)封(feng)效(xiao)果，不(bu)可超過(guo)規定(ding)(ding)之(zhi)擰(ning)(ning)緊(jin)(jin)力(li)(li)(li)矩，以(yi)防密(mi)(mi)封(feng)面(mian)被擠壞或加(jia)速磨損(sun)。注(zhu)意(yi)事(shi)(shi)項：壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)計(ji)(ji)所使(shi)(shi)(shi)用(yong)(yong)(yong)的(de)(de)(de)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)，在其(qi)標(biao)明(ming)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)的(de)(de)(de)1/2以(yi)內(nei)使(shi)(shi)(shi)用(yong)(yong)(yong)。并經常(chang)(chang)把壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)計(ji)(ji)與標(biao)準(zhun)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)計(ji)(ji)進行(xing)(xing)比(bi)較(jiao)，加(jia)以(yi)校(xiao)正。氧氣(qi)用(yong)(yong)(yong)的(de)(de)(de)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)計(ji)(ji)，要(yao)(yao)避(bi)免(mian)與其(qi)它氣(qi)體用(yong)(yong)(yong)的(de)(de)(de)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)計(ji)(ji)混用(yong)(yong)(yong)。安(an)全閥及(ji)其(qi)它的(de)(de)(de)安(an)全裝置(zhi)(zhi)，要(yao)(yao)使(shi)(shi)(shi)用(yong)(yong)(yong)經過(guo)定(ding)(ding)期檢(jian)查(cha)符合規定(ding)(ding)要(yao)(yao)求的(de)(de)(de)器械。操(cao)作(zuo)時(shi)必(bi)須注(zhu)意(yi)，溫度(du)計(ji)(ji)要(yao)(yao)準(zhun)確的(de)(de)(de)插(cha)到反(fan)(fan)應(ying)(ying)(ying)溶液中。高壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)反(fan)(fan)應(ying)(ying)(ying)釜(fu)(fu)的(de)(de)(de)操(cao)作(zuo)及(ji)注(zhu)意(yi)事(shi)(shi)項：1、高壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)反(fan)(fan)應(ying)(ying)(ying)釜(fu)(fu)應(ying)(ying)(ying)在地(di)(di)點使(shi)(shi)(shi)用(yong)(yong)(yong)，并按(an)說明(ming)書操(cao)作(zuo)。2、找出(chu)刻在主容(rong)器上的(de)(de)(de)試驗(yan)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)、使(shi)(shi)(shi)用(yong)(yong)(yong)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)和使(shi)(shi)(shi)用(yong)(yong)(yong)溫度(du)，并在其(qi)允許的(de)(de)(de)條件范圍(wei)內(nei)使(shi)(shi)(shi)用(yong)(yong)(yong)。3、壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)計(ji)(ji)使(shi)(shi)(shi)用(yong)(yong)(yong)的(de)(de)(de)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)應(ying)(ying)(ying)在標(biao)明(ming)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)的(de)(de)(de)1/2以(yi)內(nei)使(shi)(shi)(shi)用(yong)(yong)(yong)。并且經常(chang)(chang)將(jiang)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)計(ji)(ji)與標(biao)準(zhun)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)計(ji)(ji)進行(xing)(xing)比(bi)較(jiao)，進行(xing)(xing)校(xiao)正。