高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜(fu)(fu)(fu)的(de)(de)(de)(de)(de)(de)(de)操(cao)作(zuo)及注意(yi)事(shi)項：1、高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜(fu)(fu)(fu)應(ying)(ying)(ying)(ying)在(zai)(zai)(zai)地點使用(yong)(yong)(yong)，并(bing)(bing)按說明(ming)書操(cao)作(zuo)。2、找出刻(ke)在(zai)(zai)(zai)主(zhu)(zhu)容器上(shang)的(de)(de)(de)(de)(de)(de)(de)試(shi)驗(yan)(yan)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)、使用(yong)(yong)(yong)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)和使用(yong)(yong)(yong)溫(wen)度，并(bing)(bing)在(zai)(zai)(zai)其允(yun)許的(de)(de)(de)(de)(de)(de)(de)條件范圍內(nei)使用(yong)(yong)(yong)。3、壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)計(ji)使用(yong)(yong)(yong)的(de)(de)(de)(de)(de)(de)(de)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)應(ying)(ying)(ying)(ying)在(zai)(zai)(zai)標明(ming)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)的(de)(de)(de)(de)(de)(de)(de)1/2以(yi)內(nei)使用(yong)(yong)(yong)。并(bing)(bing)且(qie)經常將壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)計(ji)與標準壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)計(ji)進(jin)(jin)行比較，進(jin)(jin)行校正(zheng)。高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜(fu)(fu)(fu)有(you)哪(na)些(xie)作(zuo)用(yong)(yong)(yong)？高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜(fu)(fu)(fu)是(shi)(shi)我(wo)(wo)們(men)(men)的(de)(de)(de)(de)(de)(de)(de)主(zhu)(zhu)營產品之一(yi)，合(he)(he)(he)肥高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜(fu)(fu)(fu)，高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜(fu)(fu)(fu)從(cong)很大程度上(shang)改善(shan)了以(yi)往不能(neng)密(mi)封的(de)(de)(de)(de)(de)(de)(de)問題，而且(qie)在(zai)(zai)(zai)整(zheng)個過程當中，是(shi)(shi)沒有(you)污(wu)染(ran)的(de)(de)(de)(de)(de)(de)(de)，能(neng)夠(gou)達到特定的(de)(de)(de)(de)(de)(de)(de)高(gao)(gao)(gao)溫(wen)，高(gao)(gao)(gao)溫(wen)高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜(fu)(fu)(fu)，并(bing)(bing)能(neng)夠(gou)實(shi)現理(li)想的(de)(de)(de)(de)(de)(de)(de)反(fan)應(ying)(ying)(ying)(ying)。下(xia)(xia)面(mian)我(wo)(wo)們(men)(men)來了解一(yi)下(xia)(xia)關(guan)于高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜(fu)(fu)(fu)的(de)(de)(de)(de)(de)(de)(de)作(zuo)用(yong)(yong)(yong)方面(mian)的(de)(de)(de)(de)(de)(de)(de)知識：特別(bie)適(shi)合(he)(he)(he)使用(yong)(yong)(yong)高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜(fu)(fu)(fu)的(de)(de)(de)(de)(de)(de)(de)化學(xue)反(fan)應(ying)(ying)(ying)(ying)，是(shi)(shi)一(yi)些(xie)、或者(zhe)是(shi)(shi)有(you)毒的(de)(de)(de)(de)(de)(de)(de)反(fan)應(ying)(ying)(ying)(ying)。其還有(you)加熱的(de)(de)(de)(de)(de)(de)(de)裝置(zhi)(zhi)，可(ke)以(yi)在(zai)(zai)(zai)訂貨的(de)(de)(de)(de)(de)(de)(de)時候(hou)選擇搭配的(de)(de)(de)(de)(de)(de)(de)，并(bing)(bing)可(ke)以(yi)按照要求(qiu)來實(shi)現斧體(ti)表面(mian)的(de)(de)(de)(de)(de)(de)(de)裝置(zhi)(zhi)，讓整(zheng)個化學(xue)反(fan)應(ying)(ying)(ying)(ying)過程都是(shi)(shi)比較合(he)(he)(he)理(li)和方便的(de)(de)(de)(de)(de)(de)(de)。使用(yong)(yong)(yong)實(shi)驗(yan)(yan)室高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)(ying)(ying)釜(fu)(fu)(fu)有(you)哪(na)些(xie)注意(yi)事(shi)項:水(shui)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)試(shi)驗(yan)(yan)后，再可(ke)進(jin)(jin)密(mi)試(shi)驗(yan)(yan)。1．氣(qi)(qi)密(mi)試(shi)驗(yan)(yan)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)為我(wo)(wo)作(zuo)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)。2．氣(qi)(qi)密(mi)試(shi)驗(yan)(yan)的(de)(de)(de)(de)(de)(de)(de)介質為氮氣(qi)(qi)或者(zhe)其它惰(duo)性氣(qi)(qi)體(ti)。3．氣(qi)(qi)密(mi)試(shi)驗(yan)(yan)時，升(sheng)壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)必(bi)須(xu)分(fen)次(ci)進(jin)(jin)行。達到壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)后，保壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)一(yi)定時間(jian)，用(yong)(yong)(yong)肥皂水(shui)檢查有(you)無泄漏，合(he)(he)(he)格后緩(huan)緩(huan)泄壓(ya)(ya)(ya)(ya)(ya)(ya)(ya)(ya)。

高壓(ya)反(fan)(fan)應(ying)(ying)釜(fu)的(de)(de)操作(zuo)及(ji)(ji)注(zhu)(zhu)意事(shi)項：4、氧(yang)氣(qi)壓(ya)力計(ji)應(ying)(ying)避免與(yu)其他氣(qi)體壓(ya)力計(ji)混合。5、安全閥(fa)和(he)其他安全裝(zhuang)置應(ying)(ying)定期(qi)檢查符合要求(qiu)(qiu)的(de)(de)設(she)備(bei)。6、操作(zuo)時(shi)(shi)(shi)(shi)必須注(zhu)(zhu)意溫度(du)計(ji)應(ying)(ying)準確插(cha)入反(fan)(fan)應(ying)(ying)溶液。7、保持高壓(ya)反(fan)(fan)應(ying)(ying)釜(fu)內部和(he)墊(dian)片清(qing)潔。8、蓋(gai)(gai)上(shang)(shang)(shang)盤式法蘭蓋(gai)(gai)時(shi)(shi)(shi)(shi)，位于對(dui)角線(xian)上(shang)(shang)(shang)的(de)(de)螺栓應(ying)(ying)依次(ci)擰緊。9、測(ce)量儀器時(shi)(shi)(shi)(shi)，大(da)多(duo)數情況下(xia)玻璃表(biao)面(mian)前后兩側(ce)。所以(yi)操作(zuo)時(shi)(shi)(shi)(shi)不要站在這些危(wei)險的(de)(de)地(di)方。當預計(ji)有危(wei)險時(shi)(shi)(shi)(shi)，卸下(xia)玻璃，換(huan)上(shang)(shang)(shang)新的(de)(de)。高壓(ya)反(fan)(fan)應(ying)(ying)釜(fu)釜(fu)體材料(liao)主要采用 1cr18Ni10Ti 不銹鋼(gang)(gang)制作(zuo)，并可(ke)(ke)(ke)(ke)根據不同(tong)介質(zhi)要求(qiu)(qiu)制作(zuo)鈦材（ TA2 ）、鎳（ Ni6 ）及(ji)(ji)復(fu)合鋼(gang)(gang)板，釜(fu)體結構有平蓋(gai)(gai)、凸(tu)形蓋(gai)(gai)以(yi)及(ji)(ji)帶(dai)人孔的(de)(de)閉式反(fan)(fan)應(ying)(ying)釜(fu)體，釜(fu)蓋(gai)(gai)上(shang)(shang)(shang)的(de)(de)開孔可(ke)(ke)(ke)(ke)根據用戶(hu)要求(qiu)(qiu)進(jin)行設(she)計(ji)；加熱(re)(re)方式有夾(jia)套蒸氣(qi)、夾(jia)套熱(re)(re)油電加熱(re)(re)等形式供用戶(hu)訂貨時(shi)(shi)(shi)(shi)任意選配(pei)。 對(dui)有拋光要求(qiu)(qiu)的(de)(de)釜(fu)體內表(biao)面(mian)，可(ke)(ke)(ke)(ke)達到 以(yi)上(shang)(shang)(shang)的(de)(de)鏡面(mian)拋光水(shui)平，對(dui)高粘度(du)的(de)(de)物(wu)料(liao)加工成(cheng)錐形底，便(bian)于放料(liao)、清(qing)洗。3. 隔套上(shang)(shang)(shang)部裝(zhuang)有測(ce)速線(xian)圈(quan)，連成(cheng)一體的(de)(de)攪(jiao)(jiao)拌器與(yu)內磁環旋轉(zhuan)時(shi)(shi)(shi)(shi)，測(ce)速線(xian)圈(quan)便(bian)產生感(gan)應(ying)(ying)電動(dong)勢(shi)(shi)，該(gai)電勢(shi)(shi)與(yu)攪(jiao)(jiao)拌轉(zhuan)速相應(ying)(ying)，該(gai)電勢(shi)(shi)傳(chuan)遞到轉(zhuan)速表(biao)上(shang)(shang)(shang)，便(bian)可(ke)(ke)(ke)(ke)顯示出攪(jiao)(jiao)拌轉(zhuan)速。4. 軸承(cheng)采用不銹鋼(gang)(gang)軸承(cheng)或高強電化石墨，耐摩損，且維修周期(qi)長。

高(gao)壓(ya)反(fan)應(ying)(ying)釜的操作(zuo)及注(zhu)意(yi)事項：4、氧氣壓(ya)力計(ji)應(ying)(ying)避免與(yu)其他氣體(ti)壓(ya)力計(ji)混合。5、安全(quan)閥和其他安全(quan)裝置應(ying)(ying)定期檢查符(fu)合要(yao)求的設備(bei)。6、操作(zuo)時(shi)(shi)必須注(zhu)意(yi)溫(wen)(wen)(wen)度計(ji)應(ying)(ying)準確插(cha)(cha)入反(fan)應(ying)(ying)溶液(ye)。7、保(bao)(bao)持高(gao)壓(ya)反(fan)應(ying)(ying)釜內部(bu)和墊片清潔。8、蓋上盤式法蘭蓋時(shi)(shi)，位于對角線(xian)上的螺栓應(ying)(ying)依次擰(ning)緊。9、測量儀器(qi)時(shi)(shi)，大(da)多數情況下(xia)玻璃表面(mian)前后兩(liang)側。所以(yi)操作(zuo)時(shi)(shi)不要(yao)站在這些危險(xian)的地方(fang)。當(dang)預(yu)計(ji)有(you)(you)危險(xian)時(shi)(shi)，實驗室(shi)高(gao)壓(ya)反(fan)應(ying)(ying)釜，卸下(xia)玻璃，換(huan)上新的。5. 磁(ci)(ci)聯(lian)軸(zhou)器(qi)與(yu)釜蓋間(jian)裝有(you)(you)冷卻水套，當(dang)操作(zuo)溫(wen)(wen)(wen)度較高(gao)時(shi)(shi)應(ying)(ying)通(tong)冷卻水，以(yi)及磁(ci)(ci)鋼溫(wen)(wen)(wen)度太高(gao)而退(tui)磁(ci)(ci)。6. 聯(lian)軸(zhou)器(qi)主(zhu)(zhu)要(yao)由具(ju)有(you)(you)很強磁(ci)(ci)力的一對內、外磁(ci)(ci)環組成，高(gao)壓(ya)反(fan)應(ying)(ying)釜價格，中間(jian)有(you)(you)承壓(ya)的隔套。攪(jiao)拌(ban)器(qi)由伺(si)服(fu)電(dian)(dian)機(ji)通(tong)過(guo)聯(lian)軸(zhou)器(qi)驅(qu)動。控(kong)制(zhi)伺(si)服(fu)電(dian)(dian)機(ji)的轉(zhuan)速，便可(ke)達(da)到控(kong)制(zhi)攪(jiao)拌(ban)轉(zhuan)速的目的。使(shi)(shi)用(yong)實驗室(shi)高(gao)壓(ya)反(fan)應(ying)(ying)釜有(you)(you)哪些注(zhu)意(yi)事項:序號 故障現(xian)象 可(ke)能(neng)原因 排(pai)(pai)除方(fang)法 1 打開(kai)上電(dian)(dian)源(yuan)開(kai)關(guan)(guan)但控(kong)制(zhi)面(mian)板(ban)不亮 1.總電(dian)(dian)源(yuan)保(bao)(bao)險(xian)絲損(sun)(sun)壞(huai)。2.電(dian)(dian)源(yuan)開(kai)關(guan)(guan)內部(bu)接(jie)觸不良。3.接(jie)電(dian)(dian)電(dian)(dian)源(yuan)有(you)(you)誤。 1. 更(geng)換(huan)保(bao)(bao)險(xian)絲。2. 更(geng)換(huan)開(kai)關(guan)(guan)。3. 用(yong)表測量所使(shi)(shi)用(yong)的電(dian)(dian)源(yuan)電(dian)(dian)壓(ya)并(bing)作(zuo)更(geng)正(zheng)。 2 液(ye)晶(jing)屏上排(pai)(pai)顯(xian)示“----”， 1. 溫(wen)(wen)(wen)度傳(chuan)感(gan)器(qi)插(cha)(cha)頭沒插(cha)(cha)，2. 溫(wen)(wen)(wen)度傳(chuan)感(gan)器(qi)連(lian)接(jie)線(xian)損(sun)(sun)壞(huai)。3. 主(zhu)(zhu)板(ban)失靈(ling)。 1. 插(cha)(cha)上溫(wen)(wen)(wen)度傳(chuan)感(gan)器(qi)插(cha)(cha)頭。2. 更(geng)換(huan)溫(wen)(wen)(wen)度傳(chuan)感(gan)器(qi)連(lian)接(jie)線(xian)。3. 更(geng)換(huan)主(zhu)(zhu)板(ban)。 3 液(ye)晶(jing)屏下(xia)排(pai)(pai)顯(xian)示“E-1”且馬(ma)達(da)不工作(zuo) 1. 介(jie)質(zhi)很粘(zhan)稠(chou)至攪(jiao)拌(ban)受(shou)阻2. 軟軸(zhou)受(shou)阻 1. 檢查介(jie)質(zhi)是否(fou)很粘(zhan)稠(chou)；2. 重新拆裝軟軸(zhou)。 4 打開(kai)開(kai)關(guan)(guan)即燒(shao)(shao)保(bao)(bao)險(xian)絲或更(geng)換(huan)保(bao)(bao)險(xian)絲后馬(ma)上燒(shao)(shao)斷。 1. 加熱(re)器(qi)燒(shao)(shao)壞(huai)短(duan)路。2. 主(zhu)(zhu)板(ban)燒(shao)(shao)壞(huai) 1. 更(geng)換(huan)加熱(re)器(qi)。2. 更(geng)換(huan)主(zhu)(zhu)板(ban)。 5 溫(wen)(wen)(wen)度、攪(jiao)拌(ban)速度無法控(kong)制(zhi)。 1. 主(zhu)(zhu)板(ban)燒(shao)(shao)壞(huai)。 1.更(geng)換(huan)主(zhu)(zhu)板(ban)。