注(zhu)意(yi)事項：高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)釜(fu)(fu)屬于精密設(she)(she)備(bei)(bei)，通過密封(feng)(feng)環采(cai)用(yong)錐(zhui)面(mian)相接(jie)(jie)(jie)觸密封(feng)(feng)形(xing)式，借擰(ning)(ning)(ning)緊主螺栓使他們(men)相互壓(ya)(ya)(ya)(ya)(ya)(ya)緊而達到(dao)密封(feng)(feng)的(de)(de)目的(de)(de)。必(bi)須(xu)(xu)對(dui)密封(feng)(feng)錐(zhui)面(mian)特別加(jia)以(yi)愛(ai)護，避免各(ge)種碰(peng)撞而導致其損壞(huai)。在裝蓋(gai)時(shi)，先放置好反應(ying)釜(fu)(fu)釜(fu)(fu)體(ti)，然(ran)后將釜(fu)(fu)蓋(gai)按(an)固(gu)定位(wei)置，濟(ji)南高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)反應(ying)釜(fu)(fu)，小(xiao)心地(di)裝在釜(fu)(fu)體(ti)上，在擰(ning)(ning)(ning)緊主螺栓時(shi)，必(bi)須(xu)(xu)按(an)對(dui)角，對(dui)稱地(di)分多次逐步擰(ning)(ning)(ning)緊，用(yong)力要(yao)均勻，不(bu)允(yun)許釜(fu)(fu)蓋(gai)向一邊傾斜，小(xiao)型高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)反應(ying)釜(fu)(fu)，以(yi)達到(dao)良好的(de)(de)密封(feng)(feng)效果(guo)，不(bu)可超過規定之擰(ning)(ning)(ning)緊力矩，高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)反應(ying)釜(fu)(fu)廠家(jia)，以(yi)防密封(feng)(feng)面(mian)被擠壞(huai)或加(jia)速磨損。使用(yong)實(shi)(shi)驗(yan)(yan)(yan)室(shi)高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)反應(ying)釜(fu)(fu)有哪些(xie)(xie)注(zhu)意(yi)事項; 1.安(an)(an)(an)裝前，首先檢查各(ge)聯接(jie)(jie)(jie)件(jian)、緊固(gu)件(jian)及傳動部(bu)位(wei)是否(fou)牢(lao)固(gu)可靠。 2.安(an)(an)(an)裝時(shi)，要(yao)底座與地(di)水(shui)平(ping)垂直，不(bu)垂直度不(bu)得大(da)于設(she)(she)備(bei)(bei)總高(gao)(gao)度的(de)(de)1/1000。3.壓(ya)(ya)(ya)(ya)(ya)(ya)力表(biao)、安(an)(an)(an)全(quan)閥、法蘭(lan)等配件(jian)必(bi)須(xu)(xu)按(an)反應(ying)釜(fu)(fu)工(gong)(gong)作(zuo)壓(ya)(ya)(ya)(ya)(ya)(ya)力要(yao)求配備(bei)(bei)。4.設(she)(she)備(bei)(bei)安(an)(an)(an)放應(ying)遠(yuan)離(li)強磁場、電爐等較大(da)的(de)(de)用(yong)電設(she)(she)備(bei)(bei)。 5.檢查線(xian)路有沒(mei)有接(jie)(jie)(jie)地(di)短路等現象。6. 工(gong)(gong)作(zuo)時(shi)禁止(zhi)運輸(shu)(shu)，停止(zhi)工(gong)(gong)作(zuo)后運輸(shu)(shu)中不(bu)允(yun)許把(ba)反應(ying)器放倒或側臥(wo)運輸(shu)(shu)。組(zu)裝使用(yong)實(shi)(shi)驗(yan)(yan)(yan)室(shi)高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)反應(ying)釜(fu)(fu)有哪些(xie)(xie)注(zhu)意(yi)事項:水(shui)壓(ya)(ya)(ya)(ya)(ya)(ya)試(shi)(shi)驗(yan)(yan)(yan) 1．安(an)(an)(an)裝完畢后進行水(shui)壓(ya)(ya)(ya)(ya)(ya)(ya)試(shi)(shi)驗(yan)(yan)(yan)，水(shui)壓(ya)(ya)(ya)(ya)(ya)(ya)試(shi)(shi)驗(yan)(yan)(yan)按(an)1.05倍工(gong)(gong)作(zuo)壓(ya)(ya)(ya)(ya)(ya)(ya)力試(shi)(shi)驗(yan)(yan)(yan)。 2．要(yao)求裝配量(liang)程為工(gong)(gong)作(zuo)壓(ya)(ya)(ya)(ya)(ya)(ya)力的(de)(de)1.25倍的(de)(de)合格壓(ya)(ya)(ya)(ya)(ya)(ya)力表(biao) 3．用(yong)清潔(jie)水(shui)作(zuo)介(jie)(jie)質，確認(ren)氯離(li)子含(han)量(liang)不(bu)超過25毫(hao)克(ke)/升，不(bu)銹(xiu)鋼高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)反應(ying)釜(fu)(fu)，水(shui)溫≥5°C。4．充介(jie)(jie)質時(shi)，容器頂部(bu)設(she)(she)排(pai)氣口，必(bi)須(xu)(xu)把(ba)容器內部(bu)的(de)(de)氣體(ti)排(pai)放干(gan)凈。5．試(shi)(shi)壓(ya)(ya)(ya)(ya)(ya)(ya)時(shi)，壓(ya)(ya)(ya)(ya)(ya)(ya)力應(ying)緩慢上升，注(zhu)意(yi)觀察壓(ya)(ya)(ya)(ya)(ya)(ya)力指示是否(fou)變(bian)化，容器有無變(bian)形(xing)，傾聽(ting)有無異(yi)常聲響，達到(dao)試(shi)(shi)驗(yan)(yan)(yan)壓(ya)(ya)(ya)(ya)(ya)(ya)力保壓(ya)(ya)(ya)(ya)(ya)(ya)30分鐘(zhong)。無泄漏后，將壓(ya)(ya)(ya)(ya)(ya)(ya)力緩緩降到(dao)試(shi)(shi)驗(yan)(yan)(yan)壓(ya)(ya)(ya)(ya)(ya)(ya)力的(de)(de)80%；保壓(ya)(ya)(ya)(ya)(ya)(ya)一定時(shi)間，對(dui)所(suo)有的(de)(de)接(jie)(jie)(jie)頭和連(lian)接(jie)(jie)(jie)部(bu)位(wei)進行檢查。合格后緩緩缷壓(ya)(ya)(ya)(ya)(ya)(ya)，放盡介(jie)(jie)質，用(yong)壓(ya)(ya)(ya)(ya)(ya)(ya)縮空氣將容器內外吹干(gan)凈。

高(gao)壓反應(ying)(ying)釜(fu)(fu)(fu)的(de)特點(dian)和應(ying)(ying)用(yong)(yong)(yong)(yong)：高(gao)壓反應(ying)(ying)釜(fu)(fu)(fu)所(suo)有(you)(you)主體(ti)部(bu)件釜(fu)(fu)(fu)蓋、釜(fu)(fu)(fu)體(ti)、強(qiang)磁(ci)(ci)力(li)(li)偶(ou)合(he)攪(jiao)拌(ban)器(qi)(qi)(qi)(qi)、高(gao)溫高(gao)壓針型閥(fa)、下攪(jiao)拌(ban)部(bu)分(fen)、內(nei)(nei)冷(leng)卻盤管(guan)(guan)、測溫部(bu)分(fen)、液(ye)下管(guan)(guan)等所(suo)用(yong)(yong)(yong)(yong)材(cai)(cai)(cai)料選用(yong)(yong)(yong)(yong) 0Cr18Ni9 （ 304 ）、 1Cr18Ni9Ti （ 321 ）、 00Cr17Ni14Mo2 （ 316L / 鉬(mu)二鈦）、鈦材(cai)(cai)(cai)、哈(ha)氏(shi)合(he)金(jin) 、因考耐(nai)爾合(he)金(jin) 、鎳(nie)(nie)材(cai)(cai)(cai)、鋯(gao)材(cai)(cai)(cai)、鉭材(cai)(cai)(cai)、銀(yin)(yin)材(cai)(cai)(cai)、四氟等制成，亦可(ke)內(nei)(nei)置 316L / 鈦材(cai)(cai)(cai) / 哈(ha)氏(shi)合(he)金(jin) / 因考耐(nai)爾合(he)金(jin) / 鎳(nie)(nie)材(cai)(cai)(cai) / 鋯(gao)材(cai)(cai)(cai) / 鉭材(cai)(cai)(cai) / 銀(yin)(yin)材(cai)(cai)(cai) / 四氟等內(nei)(nei)膽(dan)、可(ke)內(nei)(nei)噴涂耐(nai)腐高(gao)溫四氟高(gao)壓反應(ying)(ying)釜(fu)(fu)(fu)的(de)操作及(ji)注意事項：1、高(gao)壓反應(ying)(ying)釜(fu)(fu)(fu)應(ying)(ying)在地點(dian)使用(yong)(yong)(yong)(yong)，并(bing)按(an)說明書操作。2、找出刻(ke)在主容器(qi)(qi)(qi)(qi)上的(de)試(shi)驗(yan)壓力(li)(li)、使用(yong)(yong)(yong)(yong)壓力(li)(li)和高(gao)使用(yong)(yong)(yong)(yong)溫度(du)，并(bing)在其允許的(de)條件范圍(wei)內(nei)(nei)使用(yong)(yong)(yong)(yong)。3、壓力(li)(li)計(ji)使用(yong)(yong)(yong)(yong)的(de)壓力(li)(li)應(ying)(ying)在標明壓力(li)(li)的(de)1/2以內(nei)(nei)使用(yong)(yong)(yong)(yong)。并(bing)且經常(chang)將壓力(li)(li)計(ji)與(yu)標準壓力(li)(li)計(ji)進(jin)(jin)行比較，進(jin)(jin)行校正。5. 磁(ci)(ci)聯(lian)軸(zhou)(zhou)器(qi)(qi)(qi)(qi)與(yu)釜(fu)(fu)(fu)蓋間(jian)裝有(you)(you)冷(leng)卻水套，當操作溫度(du)較高(gao)時應(ying)(ying)通(tong)冷(leng)卻水，以及(ji)磁(ci)(ci)鋼溫度(du)太高(gao)而退(tui)磁(ci)(ci)。6. 聯(lian)軸(zhou)(zhou)器(qi)(qi)(qi)(qi)主要由具有(you)(you)很強(qiang)磁(ci)(ci)力(li)(li)的(de)一對內(nei)(nei)、外磁(ci)(ci)環組成，中間(jian)有(you)(you)承壓的(de)隔(ge)套。攪(jiao)拌(ban)器(qi)(qi)(qi)(qi)由伺服(fu)(fu)電(dian)機(ji)通(tong)過(guo)聯(lian)軸(zhou)(zhou)器(qi)(qi)(qi)(qi)驅動。控(kong)制伺服(fu)(fu)電(dian)機(ji)的(de)轉(zhuan)速，便可(ke)達到控(kong)制攪(jiao)拌(ban)轉(zhuan)速的(de)目的(de)。

反應釜的壓力大小怎樣劃分？壓力容器按壓力大小可分為：1，低壓容器（代號L）0.1MPa≤p