使用(yong)(yong)(yong)(yong)實驗(yan)室(shi)高(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)反(fan)(fan)應(ying)釜(fu)(fu)有(you)(you)(you)(you)哪(na)些注(zhu)意(yi)事(shi)項(xiang):水(shui)壓(ya)(ya)(ya)(ya)(ya)(ya)試驗(yan) 1．安裝(zhuang)完畢后進行(xing)水(shui)壓(ya)(ya)(ya)(ya)(ya)(ya)試驗(yan)，水(shui)壓(ya)(ya)(ya)(ya)(ya)(ya)試驗(yan)按(an)1.05倍(bei)工(gong)作(zuo)(zuo)(zuo)(zuo)壓(ya)(ya)(ya)(ya)(ya)(ya)力試驗(yan)。 2．要(yao)求(qiu)裝(zhuang)配量程為工(gong)作(zuo)(zuo)(zuo)(zuo)壓(ya)(ya)(ya)(ya)(ya)(ya)力的(de)1.25倍(bei)的(de)合格(ge)(ge)壓(ya)(ya)(ya)(ya)(ya)(ya)力表(biao)(biao) 3．用(yong)(yong)(yong)(yong)清(qing)潔水(shui)作(zuo)(zuo)(zuo)(zuo)介(jie)(jie)質(zhi)(zhi)，確(que)認氯離(li)子含量不(bu)(bu)(bu)超過25毫克/升，水(shui)溫≥5°C。4．充介(jie)(jie)質(zhi)(zhi)時，容(rong)器頂部設排(pai)(pai)氣(qi)口(kou)，必須把容(rong)器內部的(de)氣(qi)體排(pai)(pai)放(fang)(fang)干凈(jing)。5．試壓(ya)(ya)(ya)(ya)(ya)(ya)時，壓(ya)(ya)(ya)(ya)(ya)(ya)力應(ying)緩慢(man)上(shang)(shang)(shang)(shang)升，注(zhu)意(yi)觀察壓(ya)(ya)(ya)(ya)(ya)(ya)力指示(shi)是(shi)否變化，容(rong)器有(you)(you)(you)(you)無(wu)(wu)變形(xing)，傾聽有(you)(you)(you)(you)無(wu)(wu)異常聲響，達到(dao)(dao)試驗(yan)壓(ya)(ya)(ya)(ya)(ya)(ya)力保壓(ya)(ya)(ya)(ya)(ya)(ya)30分鐘。無(wu)(wu)泄漏后，高(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)反(fan)(fan)應(ying)釜(fu)(fu)批(pi)發(fa)，將壓(ya)(ya)(ya)(ya)(ya)(ya)力緩緩降(jiang)到(dao)(dao)試驗(yan)壓(ya)(ya)(ya)(ya)(ya)(ya)力的(de)80%；保壓(ya)(ya)(ya)(ya)(ya)(ya)一(yi)定時間，高(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)反(fan)(fan)應(ying)釜(fu)(fu)生產廠家，對(dui)所有(you)(you)(you)(you)的(de)接(jie)頭和連接(jie)部位進行(xing)檢(jian)查(cha)。合格(ge)(ge)后緩緩缷壓(ya)(ya)(ya)(ya)(ya)(ya)，放(fang)(fang)盡介(jie)(jie)質(zhi)(zhi)，用(yong)(yong)(yong)(yong)壓(ya)(ya)(ya)(ya)(ya)(ya)縮空氣(qi)將容(rong)器內外吹干凈(jing)。高(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)反(fan)(fan)應(ying)釜(fu)(fu)釜(fu)(fu)體材料(liao)(liao)主(zhu)(zhu)要(yao)采用(yong)(yong)(yong)(yong) 1cr18Ni10Ti 不(bu)(bu)(bu)銹鋼制作(zuo)(zuo)(zuo)(zuo)，并可(ke)根據不(bu)(bu)(bu)同介(jie)(jie)質(zhi)(zhi)要(yao)求(qiu)制作(zuo)(zuo)(zuo)(zuo)鈦材（ TA2 ）、鎳（ Ni6 ）及(ji)復合鋼板(ban)(ban)(ban)，釜(fu)(fu)體結構有(you)(you)(you)(you)平蓋(gai)、凸形(xing)蓋(gai)以及(ji)帶人孔的(de)閉(bi)式(shi)(shi)反(fan)(fan)應(ying)釜(fu)(fu)體，釜(fu)(fu)蓋(gai)上(shang)(shang)(shang)(shang)的(de)開孔可(ke)根據用(yong)(yong)(yong)(yong)戶要(yao)求(qiu)進行(xing)設計；加(jia)(jia)熱(re)方式(shi)(shi)有(you)(you)(you)(you)夾(jia)套蒸氣(qi)、夾(jia)套熱(re)油電(dian)加(jia)(jia)熱(re)等形(xing)式(shi)(shi)供用(yong)(yong)(yong)(yong)戶訂貨時任意(yi)選配。 對(dui)有(you)(you)(you)(you)拋光(guang)要(yao)求(qiu)的(de)釜(fu)(fu)體內表(biao)(biao)面(mian)，可(ke)達到(dao)(dao) 以上(shang)(shang)(shang)(shang)的(de)鏡面(mian)拋光(guang)水(shui)平，對(dui)高(gao)粘度(du)的(de)物料(liao)(liao)加(jia)(jia)工(gong)成錐形(xing)底，便于(yu)放(fang)(fang)料(liao)(liao)、清(qing)洗(xi)。使用(yong)(yong)(yong)(yong)實驗(yan)室(shi)高(gao)壓(ya)(ya)(ya)(ya)(ya)(ya)反(fan)(fan)應(ying)釜(fu)(fu)有(you)(you)(you)(you)哪(na)些注(zhu)意(yi)事(shi)項(xiang):序號 故障(zhang)現(xian)象 可(ke)能原(yuan)因 排(pai)(pai)除方法(fa) 1 打(da)開上(shang)(shang)(shang)(shang)電(dian)源(yuan)(yuan)開關(guan)但控制面(mian)板(ban)(ban)(ban)不(bu)(bu)(bu)亮 1.總電(dian)源(yuan)(yuan)保險絲(si)損壞(huai)。2.電(dian)源(yuan)(yuan)開關(guan)內部接(jie)觸不(bu)(bu)(bu)良。3.接(jie)電(dian)電(dian)源(yuan)(yuan)有(you)(you)(you)(you)誤。 1. 更(geng)(geng)(geng)換保險絲(si)。2. 更(geng)(geng)(geng)換開關(guan)。3. 用(yong)(yong)(yong)(yong)表(biao)(biao)測量所使用(yong)(yong)(yong)(yong)的(de)電(dian)源(yuan)(yuan)電(dian)壓(ya)(ya)(ya)(ya)(ya)(ya)并作(zuo)(zuo)(zuo)(zuo)更(geng)(geng)(geng)正。 2 液晶屏上(shang)(shang)(shang)(shang)排(pai)(pai)顯(xian)示(shi)“----”， 1. 溫度(du)傳(chuan)感(gan)器插頭沒插，2. 溫度(du)傳(chuan)感(gan)器連接(jie)線損壞(huai)。3. 主(zhu)(zhu)板(ban)(ban)(ban)失靈。 1. 插上(shang)(shang)(shang)(shang)溫度(du)傳(chuan)感(gan)器插頭。2. 更(geng)(geng)(geng)換溫度(du)傳(chuan)感(gan)器連接(jie)線。3. 更(geng)(geng)(geng)換主(zhu)(zhu)板(ban)(ban)(ban)。 3 液晶屏下排(pai)(pai)顯(xian)示(shi)“E-1”且馬(ma)達不(bu)(bu)(bu)工(gong)作(zuo)(zuo)(zuo)(zuo) 1. 介(jie)(jie)質(zhi)(zhi)很粘稠至攪(jiao)拌(ban)受阻(zu)2. 軟軸受阻(zu) 1. 檢(jian)查(cha)介(jie)(jie)質(zhi)(zhi)是(shi)否很粘稠；2. 重新拆裝(zhuang)軟軸。 4 打(da)開開關(guan)即燒(shao)保險絲(si)或更(geng)(geng)(geng)換保險絲(si)后馬(ma)上(shang)(shang)(shang)(shang)燒(shao)斷(duan)。 1. 加(jia)(jia)熱(re)器燒(shao)壞(huai)短(duan)路。2. 主(zhu)(zhu)板(ban)(ban)(ban)燒(shao)壞(huai) 1. 更(geng)(geng)(geng)換加(jia)(jia)熱(re)器。2. 更(geng)(geng)(geng)換主(zhu)(zhu)板(ban)(ban)(ban)。 5 溫度(du)、攪(jiao)拌(ban)速度(du)無(wu)(wu)法(fa)控制。 1. 主(zhu)(zhu)板(ban)(ban)(ban)燒(shao)壞(huai)。 1.更(geng)(geng)(geng)換主(zhu)(zhu)板(ban)(ban)(ban)。

使用(yong)(yong)實驗室(shi)高(gao)(gao)(gao)(gao)壓(ya)(ya)反(fan)(fan)應(ying)(ying)(ying)釜(fu)(fu)有(you)哪(na)些(xie)(xie)注意事(shi)項; 1.安(an)(an)裝(zhuang)(zhuang)前，首(shou)先檢查各聯接件、緊(jin)(jin)固件及傳動部位是(shi)(shi)否牢固可(ke)(ke)靠。 2.安(an)(an)裝(zhuang)(zhuang)時(shi)(shi)(shi)，要(yao)(yao)底(di)座(zuo)與地水(shui)平垂直，不(bu)(bu)垂直度不(bu)(bu)得大于(yu)設(she)備總高(gao)(gao)(gao)(gao)度的(de)(de)1/1000。3.壓(ya)(ya)力表(biao)、安(an)(an)全(quan)閥、法(fa)蘭(lan)等配件必須按反(fan)(fan)應(ying)(ying)(ying)釜(fu)(fu)工作(zuo)壓(ya)(ya)力要(yao)(yao)求配備。4.設(she)備安(an)(an)放應(ying)(ying)(ying)遠離強磁場、電(dian)爐等較大的(de)(de)用(yong)(yong)電(dian)設(she)備。 5.檢查線(xian)路有(you)沒有(you)接地短路等現(xian)象(xiang)。6. 工作(zuo)時(shi)(shi)(shi)禁止(zhi)(zhi)運(yun)(yun)輸(shu)，高(gao)(gao)(gao)(gao)壓(ya)(ya)反(fan)(fan)應(ying)(ying)(ying)釜(fu)(fu)供應(ying)(ying)(ying)，停止(zhi)(zhi)工作(zuo)后運(yun)(yun)輸(shu)中不(bu)(bu)允許把反(fan)(fan)應(ying)(ying)(ying)器放倒或側臥(wo)運(yun)(yun)輸(shu)。7.組裝(zhuang)(zhuang)釜(fu)(fu)蓋時(shi)(shi)(shi)要(yao)(yao)把整個釜(fu)(fu)體(ti)脫離主機(ji)工作(zuo)，以(yi)免(mian)損壞(huai)主機(ji)，4、氧氣壓(ya)(ya)力計(ji)應(ying)(ying)(ying)避免(mian)與其他氣體(ti)壓(ya)(ya)力計(ji)混合。5、安(an)(an)全(quan)閥和(he)其他安(an)(an)全(quan)裝(zhuang)(zhuang)置(zhi)(zhi)應(ying)(ying)(ying)定(ding)期檢查符合要(yao)(yao)求的(de)(de)設(she)備。6、操作(zuo)時(shi)(shi)(shi)必須注意溫(wen)度計(ji)應(ying)(ying)(ying)準(zhun)確(que)插入反(fan)(fan)應(ying)(ying)(ying)溶液。7、保(bao)持高(gao)(gao)(gao)(gao)壓(ya)(ya)反(fan)(fan)應(ying)(ying)(ying)釜(fu)(fu)內部和(he)墊片清潔(jie)。8、蓋上盤式法(fa)蘭(lan)蓋時(shi)(shi)(shi)，位于(yu)對角線(xian)上的(de)(de)螺栓應(ying)(ying)(ying)依次擰緊(jin)(jin)。9、測量儀器時(shi)(shi)(shi)，大多數情(qing)況下玻(bo)璃(li)表(biao)面(mian)(mian)前后兩側。所以(yi)操作(zuo)時(shi)(shi)(shi)不(bu)(bu)要(yao)(yao)站在這些(xie)(xie)危(wei)險(xian)的(de)(de)地方(fang)。當(dang)預計(ji)有(you)危(wei)險(xian)時(shi)(shi)(shi)，卸下玻(bo)璃(li)，換(huan)上新的(de)(de)。高(gao)(gao)(gao)(gao)壓(ya)(ya)反(fan)(fan)應(ying)(ying)(ying)釜(fu)(fu)有(you)哪(na)些(xie)(xie)作(zuo)用(yong)(yong)？高(gao)(gao)(gao)(gao)壓(ya)(ya)反(fan)(fan)應(ying)(ying)(ying)釜(fu)(fu)是(shi)(shi)我們的(de)(de)主營(ying)產品之一，高(gao)(gao)(gao)(gao)壓(ya)(ya)反(fan)(fan)應(ying)(ying)(ying)釜(fu)(fu)從很大程度上改善了以(yi)往不(bu)(bu)能密封的(de)(de)問題，而且在整個過程當(dang)中，是(shi)(shi)沒有(you)污(wu)染的(de)(de)，能夠達(da)到特(te)定(ding)的(de)(de)高(gao)(gao)(gao)(gao)溫(wen)，并(bing)能夠實現(xian)理想的(de)(de)反(fan)(fan)應(ying)(ying)(ying)。下面(mian)(mian)我們來(lai)了解一下關于(yu)高(gao)(gao)(gao)(gao)壓(ya)(ya)反(fan)(fan)應(ying)(ying)(ying)釜(fu)(fu)的(de)(de)作(zuo)用(yong)(yong)方(fang)面(mian)(mian)的(de)(de)知識：特(te)別適合使用(yong)(yong)高(gao)(gao)(gao)(gao)壓(ya)(ya)反(fan)(fan)應(ying)(ying)(ying)釜(fu)(fu)的(de)(de)化學(xue)反(fan)(fan)應(ying)(ying)(ying)，高(gao)(gao)(gao)(gao)壓(ya)(ya)反(fan)(fan)應(ying)(ying)(ying)釜(fu)(fu)，是(shi)(shi)一些(xie)(xie)、或者是(shi)(shi)有(you)毒的(de)(de)反(fan)(fan)應(ying)(ying)(ying)。其還有(you)加(jia)熱的(de)(de)裝(zhuang)(zhuang)置(zhi)(zhi)，可(ke)(ke)以(yi)在訂貨的(de)(de)時(shi)(shi)(shi)候選擇搭配的(de)(de)，并(bing)可(ke)(ke)以(yi)按照要(yao)(yao)求來(lai)實現(xian)斧體(ti)表(biao)面(mian)(mian)的(de)(de)裝(zhuang)(zhuang)置(zhi)(zhi)，讓整個化學(xue)反(fan)(fan)應(ying)(ying)(ying)過程都是(shi)(shi)比較合理和(he)方(fang)便的(de)(de)。

3. 隔套上部裝有(you)測速(su)線圈，連成一體(ti)的(de)(de)(de)攪拌器與(yu)內(nei)磁環旋轉(zhuan)(zhuan)時(shi)，測速(su)線圈便產生感應(ying)電動勢(shi)，該電勢(shi)與(yu)攪拌轉(zhuan)(zhuan)速(su)相應(ying)，該電勢(shi)傳遞到轉(zhuan)(zhuan)速(su)表(biao)上，便可(ke)顯示出攪拌轉(zhuan)(zhuan)速(su)。4. 軸(zhou)(zhou)承采用(yong)(yong)(yong)不(bu)銹(xiu)鋼軸(zhou)(zhou)承或高(gao)強電化石墨，耐摩損，且(qie)維修(xiu)周期長。高(gao)壓(ya)(ya)(ya)(ya)反應(ying)釜(fu)(fu)(fu)(fu)的(de)(de)(de)操作(zuo)及(ji)注意事(shi)項(xiang)：1、高(gao)壓(ya)(ya)(ya)(ya)反應(ying)釜(fu)(fu)(fu)(fu)應(ying)在地點使用(yong)(yong)(yong)，并按(an)說(shuo)明書操作(zuo)。2、找出刻(ke)在主(zhu)容器上的(de)(de)(de)試驗壓(ya)(ya)(ya)(ya)力(li)、使用(yong)(yong)(yong)壓(ya)(ya)(ya)(ya)力(li)和高(gao)使用(yong)(yong)(yong)溫度，并在其允許的(de)(de)(de)條件(jian)范圍內(nei)使用(yong)(yong)(yong)。3、壓(ya)(ya)(ya)(ya)力(li)計(ji)使用(yong)(yong)(yong)的(de)(de)(de)壓(ya)(ya)(ya)(ya)力(li)應(ying)在標明壓(ya)(ya)(ya)(ya)力(li)的(de)(de)(de)1/2以內(nei)使用(yong)(yong)(yong)。并且(qie)經常將壓(ya)(ya)(ya)(ya)力(li)計(ji)與(yu)標準壓(ya)(ya)(ya)(ya)力(li)計(ji)進(jin)行比較，進(jin)行校正。高(gao)壓(ya)(ya)(ya)(ya)反應(ying)釜(fu)(fu)(fu)(fu)釜(fu)(fu)(fu)(fu)體(ti)材料(liao)主(zhu)要(yao)采用(yong)(yong)(yong) 1cr18Ni10Ti 不(bu)銹(xiu)鋼制(zhi)作(zuo)，并可(ke)根(gen)據(ju)不(bu)同介質(zhi)要(yao)求制(zhi)作(zuo)鈦材（ TA2 ）、鎳（ Ni6 ）及(ji)復合鋼板，釜(fu)(fu)(fu)(fu)體(ti)結構有(you)平蓋、凸形蓋以及(ji)帶人孔(kong)的(de)(de)(de)閉式(shi)反應(ying)釜(fu)(fu)(fu)(fu)體(ti)，釜(fu)(fu)(fu)(fu)蓋上的(de)(de)(de)開孔(kong)可(ke)根(gen)據(ju)用(yong)(yong)(yong)戶要(yao)求進(jin)行設計(ji)；加熱(re)方式(shi)有(you)夾(jia)套蒸氣、夾(jia)套熱(re)油電加熱(re)等形式(shi)供用(yong)(yong)(yong)戶訂貨(huo)時(shi)任意選配。 對(dui)有(you)拋光要(yao)求的(de)(de)(de)釜(fu)(fu)(fu)(fu)體(ti)內(nei)表(biao)面，可(ke)達到 以上的(de)(de)(de)鏡(jing)面拋光水(shui)平，對(dui)高(gao)粘度的(de)(de)(de)物料(liao)加工成錐形底，便于放料(liao)、清(qing)洗(xi)。