使(shi)(shi)用(yong)(yong)實驗(yan)室高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)釜(fu)(fu)有(you)(you)哪些注(zhu)(zhu)意(yi)事項(xiang):水(shui)(shui)壓(ya)(ya)(ya)(ya)(ya)試驗(yan) 1．安裝完畢后(hou)進(jin)行水(shui)(shui)壓(ya)(ya)(ya)(ya)(ya)試驗(yan)，水(shui)(shui)壓(ya)(ya)(ya)(ya)(ya)試驗(yan)按1.05倍工作(zuo)壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)試驗(yan)。 2．要(yao)求(qiu)(qiu)裝配量(liang)程為工作(zuo)壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)的(de)(de)(de)1.25倍的(de)(de)(de)合格(ge)(ge)壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)表(biao) 3．用(yong)(yong)清(qing)(qing)潔(jie)(jie)水(shui)(shui)作(zuo)介質，確認氯(lv)離(li)子(zi)含量(liang)不(bu)超過25毫(hao)克/升(sheng)，水(shui)(shui)溫(wen)≥5°C。4．充介質時，容器(qi)(qi)頂部(bu)設排氣(qi)口，必(bi)須(xu)把容器(qi)(qi)內(nei)(nei)部(bu)的(de)(de)(de)氣(qi)體排放(fang)干凈。5．試壓(ya)(ya)(ya)(ya)(ya)時，壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)應(ying)(ying)緩(huan)(huan)慢上(shang)升(sheng)，注(zhu)(zhu)意(yi)觀察(cha)壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)指示是否變化，高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)釜(fu)(fu)，容器(qi)(qi)有(you)(you)無變形(xing)，傾聽有(you)(you)無異常(chang)聲(sheng)響，達到(dao)(dao)試驗(yan)壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)保壓(ya)(ya)(ya)(ya)(ya)30分鐘。無泄漏后(hou)，將壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)緩(huan)(huan)緩(huan)(huan)降到(dao)(dao)試驗(yan)壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)的(de)(de)(de)80%；保壓(ya)(ya)(ya)(ya)(ya)一定(ding)時間，高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)釜(fu)(fu)廠商，對所有(you)(you)的(de)(de)(de)接(jie)頭和連接(jie)部(bu)位進(jin)行檢查。合格(ge)(ge)后(hou)緩(huan)(huan)緩(huan)(huan)缷(xie)壓(ya)(ya)(ya)(ya)(ya)，放(fang)盡介質，用(yong)(yong)壓(ya)(ya)(ya)(ya)(ya)縮(suo)空氣(qi)將容器(qi)(qi)內(nei)(nei)外(wai)吹干凈。注(zhu)(zhu)意(yi)事項(xiang)：高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)釜(fu)(fu)要(yao)在的(de)(de)(de)地點使(shi)(shi)用(yong)(yong)，并按照使(shi)(shi)用(yong)(yong)說明進(jin)行操作(zuo)。查明刻于主體容器(qi)(qi)上(shang)的(de)(de)(de)試驗(yan)壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)、使(shi)(shi)用(yong)(yong)壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)及使(shi)(shi)用(yong)(yong)溫(wen)度等條件，要(yao)在其(qi)容許的(de)(de)(de)條件范圍內(nei)(nei)進(jin)行使(shi)(shi)用(yong)(yong)。高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)釜(fu)(fu)的(de)(de)(de)操作(zuo)及注(zhu)(zhu)意(yi)事項(xiang)：4、氧氣(qi)壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)計(ji)(ji)應(ying)(ying)避免與其(qi)他氣(qi)體壓(ya)(ya)(ya)(ya)(ya)力(li)(li)(li)(li)計(ji)(ji)混合。5、安全閥和其(qi)他安全裝置(zhi)應(ying)(ying)定(ding)期檢查符(fu)合要(yao)求(qiu)(qiu)的(de)(de)(de)設備。6、操作(zuo)時必(bi)須(xu)注(zhu)(zhu)意(yi)溫(wen)度計(ji)(ji)應(ying)(ying)準確插入反(fan)應(ying)(ying)溶液(ye)。7、保持(chi)高(gao)(gao)壓(ya)(ya)(ya)(ya)(ya)反(fan)應(ying)(ying)釜(fu)(fu)內(nei)(nei)部(bu)和墊片(pian)清(qing)(qing)潔(jie)(jie)。8、蓋上(shang)盤式法蘭蓋時，位于對角線上(shang)的(de)(de)(de)螺栓應(ying)(ying)依次(ci)擰緊。9、測量(liang)儀器(qi)(qi)時，大多數情況下玻璃表(biao)面前后(hou)兩側。所以操作(zuo)時不(bu)要(yao)站(zhan)在這些危險的(de)(de)(de)地方。當預計(ji)(ji)有(you)(you)危險時，卸下玻璃，換上(shang)新的(de)(de)(de)。

3. 隔套(tao)上(shang)部裝有測速(su)線(xian)圈(quan)(quan)，連成一體(ti)(ti)的(de)(de)(de)攪(jiao)拌(ban)器與內(nei)磁環旋轉(zhuan)時，測速(su)線(xian)圈(quan)(quan)便產生感應電動勢(shi)，該(gai)電勢(shi)與攪(jiao)拌(ban)轉(zhuan)速(su)相(xiang)應，該(gai)電勢(shi)傳遞到轉(zhuan)速(su)表上(shang)，便可顯示出(chu)攪(jiao)拌(ban)轉(zhuan)速(su)。4. 軸(zhou)(zhou)承采用(yong)(yong)(yong)(yong)不(bu)銹鋼(gang)軸(zhou)(zhou)承或高(gao)(gao)(gao)強電化石墨(mo)，耐摩(mo)損，且維修周期(qi)長。高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)反應釜(fu)的(de)(de)(de)操作及(ji)注意事項：1、高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)反應釜(fu)應在地點使(shi)用(yong)(yong)(yong)(yong)，并按說明書操作。2、找出(chu)刻(ke)在主容(rong)器上(shang)的(de)(de)(de)試驗(yan)壓(ya)(ya)(ya)(ya)力(li)、使(shi)用(yong)(yong)(yong)(yong)壓(ya)(ya)(ya)(ya)力(li)和(he)高(gao)(gao)(gao)使(shi)用(yong)(yong)(yong)(yong)溫度(du)，并在其允許的(de)(de)(de)條件范圍內(nei)使(shi)用(yong)(yong)(yong)(yong)。3、壓(ya)(ya)(ya)(ya)力(li)計(ji)使(shi)用(yong)(yong)(yong)(yong)的(de)(de)(de)壓(ya)(ya)(ya)(ya)力(li)應在標明壓(ya)(ya)(ya)(ya)力(li)的(de)(de)(de)1/2以(yi)內(nei)使(shi)用(yong)(yong)(yong)(yong)。并且經(jing)常將壓(ya)(ya)(ya)(ya)力(li)計(ji)與標準(zhun)壓(ya)(ya)(ya)(ya)力(li)計(ji)進(jin)(jin)行比較，大型高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)反應釜(fu)，進(jin)(jin)行校正。高(gao)(gao)(gao)壓(ya)(ya)(ya)(ya)反應釜(fu)釜(fu)體(ti)(ti)材料主要(yao)采用(yong)(yong)(yong)(yong) 1cr18Ni10Ti 不(bu)銹鋼(gang)制作，并可根據不(bu)同(tong)介質要(yao)求(qiu)(qiu)制作鈦材（ TA2 ）、鎳（ Ni6 ）及(ji)復合鋼(gang)板(ban)，釜(fu)體(ti)(ti)結構有平蓋、凸(tu)形蓋以(yi)及(ji)帶(dai)人(ren)孔的(de)(de)(de)閉(bi)式(shi)反應釜(fu)體(ti)(ti)，釜(fu)蓋上(shang)的(de)(de)(de)開孔可根據用(yong)(yong)(yong)(yong)戶(hu)要(yao)求(qiu)(qiu)進(jin)(jin)行設計(ji)；加熱(re)方式(shi)有夾套(tao)蒸氣、夾套(tao)熱(re)油電加熱(re)等(deng)形式(shi)供用(yong)(yong)(yong)(yong)戶(hu)訂貨時任意選配。 對(dui)有拋光要(yao)求(qiu)(qiu)的(de)(de)(de)釜(fu)體(ti)(ti)內(nei)表面(mian)，可達到 以(yi)上(shang)的(de)(de)(de)鏡(jing)面(mian)拋光水平，對(dui)高(gao)(gao)(gao)粘度(du)的(de)(de)(de)物料加工成錐形底(di)，便于放料、清洗。

使(shi)(shi)用(yong)(yong)實(shi)驗室高(gao)(gao)(gao)壓(ya)(ya)反(fan)(fan)(fan)應(ying)釜(fu)有(you)(you)哪些注意(yi)(yi)事項(xiang)(xiang)：前用(yong)(yong)軟布(bu)擦干(gan)凈，不(bu)能(neng)有(you)(you)雜質影響密(mi)(mi)(mi)(mi)封(feng)(feng)，操作(zuo)(zuo)時(shi)(shi)要(yao)注意(yi)(yi)保(bao)護(hu)上(shang)緊(jin)(jin)主螺栓(shuan)(shuan)時(shi)(shi)不(bu)可(ke)用(yong)(yong)力(li)過猛，不(bu)得(de)(de)超(chao)過擰緊(jin)(jin)力(li)矩(ju)范圍80~120N.M；且應(ying)按(an)對角分布(bu)原則，均勻對稱地(di)上(shang)緊(jin)(jin)螺栓(shuan)(shuan)，分2~3次擰緊(jin)(jin)，以防(fang)止擠壞密(mi)(mi)(mi)(mi)封(feng)(feng)面。組(zu)裝(zhuang)(zhuang)時(shi)(shi)，要(yao)輕(qing)拿輕(qing)放(fang)，防(fang)止密(mi)(mi)(mi)(mi)封(feng)(feng)面相互撞擊，不(bu)允(yun)許硬物(wu)碰(peng)撞密(mi)(mi)(mi)(mi)封(feng)(feng)部分，以免損壞密(mi)(mi)(mi)(mi)封(feng)(feng)面而(er)導(dao)致(zhi)泄漏(lou)。若使(shi)(shi)用(yong)(yong)合理(li)，可(ke)使(shi)(shi)用(yong)(yong)千次以上(shang)。密(mi)(mi)(mi)(mi)封(feng)(feng)面損傷后(hou)，要(yao)重新(xin)整修(xiu)拋光后(hou)，方可(ke)恢(hui)復密(mi)(mi)(mi)(mi)封(feng)(feng)性(xing)能(neng)。上(shang)述工(gong)作(zuo)(zuo)完成后(hou)，按(an)設計壓(ya)(ya)力(li)進行水(shui)壓(ya)(ya)試(shi)驗與(yu)氣(qi)(qi)密(mi)(mi)(mi)(mi)性(xing)試(shi)驗，介(jie)質為去離子水(shui)、氮(dan)氣(qi)(qi)或(huo)者其它(ta)惰性(xing)氣(qi)(qi)體，嚴(yan)禁使(shi)(shi)用(yong)(yong)氣(qi)(qi)體，升壓(ya)(ya)必(bi)須(xu)分次進行，保(bao)壓(ya)(ya)15~30分鐘，不(bu)得(de)(de)有(you)(you)泄漏(lou)，發現(xian)漏(lou)氣(qi)(qi)應(ying)后(hou)修(xiu)復再試(shi)驗。高(gao)(gao)(gao)壓(ya)(ya)反(fan)(fan)(fan)應(ying)釜(fu)有(you)(you)哪些作(zuo)(zuo)用(yong)(yong)？高(gao)(gao)(gao)壓(ya)(ya)反(fan)(fan)(fan)應(ying)釜(fu)的(de)出(chu)現(xian)，能(neng)夠(gou)幫助到(dao)很多實(shi)驗的(de)過程(cheng)，也能(neng)夠(gou)實(shi)現(xian)不(bu)同的(de)物(wu)質混合而(er)產生一些技術(shu)，能(neng)夠(gou)給企業或(huo)單位(wei)，帶(dai)來的(de)財富與(yu)上(shang)級。高(gao)(gao)(gao)壓(ya)(ya)反(fan)(fan)(fan)應(ying)裝(zhuang)(zhuang)置再加上(shang)刺(ci)激(ji)傳動(dong)裝(zhuang)(zhuang)置，能(neng)夠(gou)在實(shi)現(xian)的(de)效果，給整個實(shi)驗的(de)過程(cheng)帶(dai)來更多的(de)安全(quan)性(xing)和可(ke)靠性(xing)的(de)。使(shi)(shi)用(yong)(yong)實(shi)驗室高(gao)(gao)(gao)壓(ya)(ya)反(fan)(fan)(fan)應(ying)釜(fu)有(you)(you)哪些注意(yi)(yi)事項(xiang)(xiang); 1.安裝(zhuang)(zhuang)前，首(shou)先檢查各聯接件、緊(jin)(jin)固(gu)件及(ji)傳動(dong)部位(wei)是否(fou)牢固(gu)可(ke)靠。 2.安裝(zhuang)(zhuang)時(shi)(shi)，光催化高(gao)(gao)(gao)壓(ya)(ya)反(fan)(fan)(fan)應(ying)釜(fu)，要(yao)底座與(yu)地(di)水(shui)平垂(chui)直，不(bu)垂(chui)直度不(bu)得(de)(de)大于設備(bei)(bei)總高(gao)(gao)(gao)度的(de)1/1000。3.壓(ya)(ya)力(li)表(biao)、安全(quan)閥、法蘭(lan)等配件必(bi)須(xu)按(an)反(fan)(fan)(fan)應(ying)釜(fu)工(gong)作(zuo)(zuo)壓(ya)(ya)力(li)要(yao)求配備(bei)(bei)。4.設備(bei)(bei)安放(fang)應(ying)遠離強(qiang)磁場、電爐等較(jiao)大的(de)用(yong)(yong)電設備(bei)(bei)。 5.檢查線路有(you)(you)沒有(you)(you)接地(di)短路等現(xian)象。6. 工(gong)作(zuo)(zuo)時(shi)(shi)禁止運輸(shu)，停止工(gong)作(zuo)(zuo)后(hou)運輸(shu)中不(bu)允(yun)許把反(fan)(fan)(fan)應(ying)器(qi)放(fang)倒(dao)或(huo)側臥運輸(shu)。